Keyword: target
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SUPFDV009 Thermal Annealing of Sputtered Nb3Sn and V3Si Thin Films for Superconducting RF Cavities SRF, cavity, ECR, radio-frequency 82
 
  • K. Howard, M. Liepe, Z. Sun
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
 
  Funding: U.S. National Science Foundation under Award PHY-1549132, the Center for Bright Beams and Cornell Center for Materials Research Shared Facilities supported through the NSF MRSEC program (DMR-1719875)
Nb3Sn and V3Si thin films are alternative material candidates for the next-generation of superconducting radio frequency (SRF) cavities. However, past sputtered films suffer from stoichiometry and strain issues during deposition and post annealing. As such, we aim to explore the structural and chemical effects of thermal annealing, both in-situ and post-sputtering, on DC-sputtered Nb3Sn and V3Si with varying thickness on Nb or Cu substrates. We successfully enabled recrystallization of 100 nm thin Nb3Sn films with stoichiometric and strain-free grains at 950 C annealing. For 2 um films, we observed removal of strain and slight increase in grain size with increasing temperature. A phase transformation from unstable to stable structure appeared on thick V3Si samples, while we observed significant Sn loss in thick Nb3Sn films at high temperature anneals. For films on Cu substrates, we observed similar Sn and Si loss during annealing likely due to Cu-Sn and Cu-Si phase generation and subsequent Sn and Si evaporation. These results encourage us to refine our process to obtain high quality films for SRF use.
 
DOI • reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2021-SUPFDV009  
About • Received ※ 22 June 2021 — Revised ※ 06 July 2021 — Accepted ※ 12 August 2021 — Issue date ※ 17 March 2022
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TUPCAV006 Nb3Sn Films Depositions from Targets Synthesized via Liquid Tin Diffusion niobium, cavity, controls, site 452
 
  • M. Zanierato, O. Azzolini, E. Chyhyrynets, V.A. Garcia Diaz, G. Keppel, C. Pira, F. Stivanello
    INFN/LNL, Legnaro (PD), Italy
 
  The deposition of Nb3Sn on copper cavities is inter-esting for the higher thermal conductivity of copper compared to common Nb substrates. The better heat exchange would allow the use of cryocoolers reducing cryogenic costs and the risk of thermal quench [1]. Magnetron sputtering technology allows the deposi-tion of Nb3Sn on substrates different than Nb, however the coating of substrates with complex geometry (such as elliptical cavities) may require targets with non-planar shape, difficult to realize with classic powder sintering techniques. In this work, the possibility of using the Liquid Tin Diffusion (LTD) technique to produce sputtering targets is explored. The LTD tech-nique is a wire fabrication technology, already devel-oped in the past at LNL for SRF applications [2], that allows the deposition of very thick and uniform coat-ing on Nb substrates even with complex geometry [3]. Improvements in LTD process, proof of concept of a single use LTD target production, and characterization of the Nb3Sn film coated by DC magnetron sputtering with these innovative targets are reported in this work.  
poster icon Poster TUPCAV006 [5.032 MB]  
DOI • reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2021-TUPCAV006  
About • Received ※ 21 June 2021 — Revised ※ 12 July 2021 — Accepted ※ 23 August 2021 — Issue date ※ 02 September 2021
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THPCAV014 Development of High-Q Treatments for PIP-II Prototype Cavities at LASA-INFN cavity, SRF, niobium, operation 820
 
  • M. Bertucci, A. Bosotti, A. D’Ambros, A.T. Grimaldi, P. Michelato, L. Monaco, C. Pagani, R. Paparella, D. Sertore
    INFN/LASA, Segrate (MI), Italy
  • A. Gresele, A. Torri
    Ettore Zanon S.p.A., Nuclear Division, Schio, Italy
  • C. Pagani
    Università degli Studi di Milano & INFN, Segrate, Italy
  • M. Rizzi
    Ettore Zanon S.p.A., Schio, Italy
 
  INFN-LASA is currently involved in the production of PIP-II low-beta cavity prototypes. The main challenge of this activity is to develop a state-of-the art surface treatment recipe on such cavity geometry, to achieve the high-Q target required for cavity operation in the linac. This paper reports the status of cavity treatments development and the first cold test results of a single-cell cavity. This cavity has undergone a baseline treatment based on Electropolishing as bulk removal step. Being this test successful, a strategy for pushing the cavities towards higher performances is here proposed.  
DOI • reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2021-THPCAV014  
About • Received ※ 21 June 2021 — Accepted ※ 01 March 2022 — Issue date; ※ 01 May 2022  
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THPTEV015 Cylindrical Magnetron Development for Nb3sn Deposition via Magnetron Sputtering cavity, SRF, site, radio-frequency 868
 
  • Md.N. Sayeed, H. Elsayed-Ali
    ODU, Norfolk, Virginia, USA
  • C. Côté, M.A. Farzad, A. Sarkissian
    PLASMIONIQUE Inc., Varennes, Québec, Canada
  • G.V. Eremeev
    Fermilab, Batavia, Illinois, USA
  • A-M. Valente-Feliciano
    JLab, Newport News, Virginia, USA
 
  Funding: This work was supported by the U.S. Department of Energy, Office of Science, Office of Nuclear Physics under Contract No. DE-AC05-06OR23177.
Due to its better superconducting properties (critical temperature Tc~ 18.3 K, superheating field Hsh~ 400 mT), Nb3Sn is considered as a potential alternative to niobium (Tc~ 9.25 K, Hsh~ 200 mT) for superconducting radiofrequency (SRF) cavities for particle acceleration. Magnetron sputtering is an effective method to produce superconducting Nb3Sn films. We deposited superconducting Nb3Sn films on samples with magnetron sputtering using co-sputtering, sequential sputtering, and sputtering from a stoichiometric target. Nb3Sn films produced by magnetron sputtering in our previous experiments have achieved DC superconducting critical temperature up to 17.93 K and RF superconducting transition at 17.2 K. A magnetron sputtering system with two identical cylindrical cathodes that can be used to sputter Nb3Sn films on cavities has been designed and is under development now. We report on the design and the current progress on the development of the system.
 
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DOI • reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2021-THPTEV015  
About • Received ※ 22 June 2021 — Revised ※ 12 August 2021 — Accepted ※ 21 August 2021 — Issue date ※ 27 September 2021
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FROFDV06 Synthesis of Nb and Alternative Superconducting Film to Nb for SRF Cavity as Single Layer site, cavity, SRF, niobium 893
 
  • R. Valizadeh, P. Goudket, A.N. Hannah, O.B. Malyshev
    STFC/DL/ASTeC, Daresbury, Warrington, Cheshire, United Kingdom
  • C.Z. Antoine
    CEA-DRF-IRFU, France
  • C.Z. Antoine
    CEA-IRFU, Gif-sur-Yvette, France
  • E. Chyhyrynets, C. Pira
    INFN/LNL, Legnaro (PD), Italy
  • P. Goudket, O.B. Malyshev, D.J. Seal, B.S. Sian, D.A. Turner
    Cockcroft Institute, Warrington, Cheshire, United Kingdom
  • O. Kugeler, D.B. Tikhonov
    HZB, Berlin, Germany
  • S.B. Leith, A.O. Sezgin, M. Vogel
    University Siegen, Siegen, Germany
  • A. Medvids, P. Onufrijevs
    Riga Technical University, Riga, Latvia
  • D.J. Seal, B.S. Sian, D.A. Turner
    Lancaster University, Lancaster, United Kingdom
  • G.B.G. Stenning
    STFC/RAL/ISIS, Chilton, Didcot, Oxon, United Kingdom
  • A. Sublet, G. Vandoni, L. Vega Cid, W. Venturini Delsolaro, P. Vidal Garcia
    CERN, Meyrin, Switzerland
 
  "Bulk niobium (Nb) has been the material of choice for superconducting RF (SRF) cavities but for further improvement in cavity RF performance, one may have to turn to films of Nb and to other superconducting materials deposited on copper as thermal and mechanical support. Other materials known as A15, such as Nb3Sn or V3Si and B1 such as NbTiN and NbN are much easier to synthesise in thin films rather than being made as bulk cavity. The potential benefits of using materials other than Nb would be a higher Tc, a potentially higher critical held Hc, leading to potentially significant cryogenics cost reduction if the cavity operation temperature is 4.2 K or higher. We report on optimising deposition parameters and effect of substrate treatment prior to deposition for successful synthesising of Nb and the alternative superconducting thin film with high superconducting properties (Tc and Hsh) on flat substrates and QPR samples in single layer. The DC and RF SC properties have been tested using PPMS and QPR measurements. This work is part of the H2020 ARIES collaboration. We further report on preparation of RF cavities employing these alternative material for future cavity production."  
DOI • reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2021-FROFDV06  
About • Received ※ 21 June 2021 — Accepted ※ 05 January 2022 — Issue date; ※ 28 April 2022  
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